Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2015-06-02 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.97923 |
| Spacegroup name | I 41 |
| Unit cell lengths | 162.210, 162.210, 76.150 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 38.730 - 1.950 |
| R-factor | 0.1836 |
| Rwork | 0.181 |
| R-free | 0.22986 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3m22 |
| RMSD bond length | 0.019 |
| RMSD bond angle | 2.166 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.090 | 2.060 |
| High resolution limit [Å] | 1.950 | 1.950 |
| Number of reflections | 71979 | |
| <I/σ(I)> | 11.9 | |
| Completeness [%] | 99.9 | |
| Redundancy | 5.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 291 | 30% PEG 4000, 0.1 M Tris-HCl, 0.2 M Li2SO4 |
