5JIA
The Crystal Structure Of IUS-SPRY Domain From RanBP10
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-01-20 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.00000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 146.340, 79.240, 157.630 |
Unit cell angles | 90.00, 97.91, 90.00 |
Refinement procedure
Resolution | 41.250 - 1.800 |
R-factor | 0.184 |
Rwork | 0.184 |
R-free | 0.22700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5ji7 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.194 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.081 | 0.272 |
Number of reflections | 330519 | |
<I/σ(I)> | 14.159 | 2.563 |
Completeness [%] | 92.6 | 85.2 |
Redundancy | 4.1 | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9 | 295 | 0.1M BICINE, PH 9.0, 10% PEG 20000, 0- 2% DIOXANE, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 295K |