5JEX
Crystal structure of type 2 PDF from Streptococcus agalactiae, crystallized in imidazole buffer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-12-01 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9755 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.320, 65.550, 88.710 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.370 - 2.000 |
R-factor | 0.16116 |
Rwork | 0.159 |
R-free | 0.20774 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2aie |
RMSD bond length | 0.014 |
RMSD bond angle | 1.557 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.120 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 16886 | |
<I/σ(I)> | 17.04 | 6.63 |
Completeness [%] | 99.9 | 99.3 |
Redundancy | 7.1 | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 7% PEG-8000 , 100mM Imidazole pH7.5, 300mM Zn Acetate |