5JDR
Structure of PD-L1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2015-05-24 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.9791 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 72.240, 91.510, 141.830 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 70.920 - 2.700 |
| R-factor | 0.22998 |
| Rwork | 0.227 |
| R-free | 0.27558 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4z18 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.188 |
| Data reduction software | iMOSFLM |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 70.920 |
| High resolution limit [Å] | 2.700 |
| Number of reflections | 13282 |
| <I/σ(I)> | 10.8 |
| Completeness [%] | 99.9 |
| Redundancy | 6.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | LIQUID DIFFUSION | 295 | 0.2 M Ammonium Acetate, 20% PEG 3350 |
