5JDJ
Crystal structure of domain I10 from titin in space group P212121
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-06-28 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.9173 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 74.637, 136.239, 140.095 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.652 - 1.738 |
R-factor | 0.1864 |
Rwork | 0.186 |
R-free | 0.22420 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.115 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.652 | 1.800 |
High resolution limit [Å] | 1.738 | 1.738 |
Number of reflections | 145378 | |
<I/σ(I)> | 15.38 | 2.77 |
Completeness [%] | 98.8 | 95.19 |
Redundancy | 7.5 | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 292 | 0.2 M CaCl2, 0.1 M Tris pH 7.5, 25% [w/v] PEG 8000 |