5JCD
Crystal structure of OsCEBiP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2015-09-06 |
| Detector | AGILENT EOS CCD |
| Wavelength(s) | 1 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 47.772, 77.274, 111.391 |
| Unit cell angles | 90.00, 99.02, 90.00 |
Refinement procedure
| Resolution | 29.600 - 2.400 |
| R-factor | 0.223 |
| Rwork | 0.220 |
| R-free | 0.27600 |
| Structure solution method | SAD |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.403 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SHELXD |
| Refinement software | PHENIX (1.8_1069) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.600 | 2.480 |
| High resolution limit [Å] | 2.390 | 2.400 |
| Number of reflections | 31051 | |
| <I/σ(I)> | 22 | |
| Completeness [%] | 98.3 | |
| Redundancy | 4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 292 | 0.2 M ammonium acetate, 0.1 M sodium acetate trihydrate, 30%(w/v) PEG4000 |
