5ICK
A unique binding model of FXR LBD with feroline
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 293.15 |
| Detector technology | CCD |
| Collection date | 2013-03-11 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.0050 |
| Spacegroup name | P 1 2 1 |
| Unit cell lengths | 56.161, 34.910, 134.915 |
| Unit cell angles | 90.00, 90.51, 90.00 |
Refinement procedure
| Resolution | 50.010 - 2.470 |
| R-factor | 0.2155 |
| Rwork | 0.212 |
| R-free | 0.27710 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 2.040 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 134.910 |
| High resolution limit [Å] | 2.470 |
| Number of reflections | 19055 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 20% polyethylene glycol 3350 and 0.2 M ammonia acetate |
