Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 120 |
| Detector technology | CCD |
| Collection date | 2005-01-20 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 1.3861 |
| Spacegroup name | P 6 2 2 |
| Unit cell lengths | 120.510, 120.510, 183.130 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 14.942 - 3.000 |
| R-factor | 0.1841 |
| Rwork | 0.181 |
| R-free | 0.23950 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2CMZ |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.907 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.000 | 3.200 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.110 | 0.500 |
| Number of reflections | 16104 | |
| <I/σ(I)> | 6.6 | 1.7 |
| Completeness [%] | 97.5 | 94.6 |
| Redundancy | 2 | 1.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.7 | 293 | 0.1M TRIS PH 8.7, NANO3 0.4M, PEG 4000 24% |
