5HZR

Crystal structure of MtSnf2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	173
Detector technology	CCD
Collection date	2015-02-18
Detector	ADSC QUANTUM 315
Wavelength(s)	0.987
Spacegroup name	C 2 2 21
Unit cell lengths	122.613, 144.266, 121.290
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	44.769 - 2.330
R-factor	0.1953
Rwork	0.194
R-free	0.21310
RMSD bond length	0.004
RMSD bond angle	0.715
Data reduction software	HKL-2000 (V705)
Data scaling software	HKL-2000 (V705)
Phasing software	PHASER
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	62.000
High resolution limit [Å]	2.300
Number of reflections	41149
<I/σ(I)>	24.6
Completeness [%]	85.7
Redundancy	5.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION		277	ammonium sulfate, protamine, NDSB-221