5HPH
Structure of TRAP1 fragment
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 93 |
Detector technology | CCD |
Collection date | 2015-04-26 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97929 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 93.437, 104.946, 156.909 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.764 - 2.429 |
R-factor | 0.1966 |
Rwork | 0.195 |
R-free | 0.23790 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.035 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.10_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.764 | 2.470 |
High resolution limit [Å] | 2.429 | 2.430 |
Number of reflections | 58241 | |
<I/σ(I)> | 10.6 | |
Completeness [%] | 99.0 | 90.7 |
Redundancy | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.25 | 287 | 1.8M Ammonium Sulfate, 0.1M MES, 1% dioxane |