5HP7
Crystal structures of RidA in the apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | Agilent SuperNova |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-09-17 |
Detector | OXFORD ONYX CCD |
Wavelength(s) | 1.54 |
Spacegroup name | H 3 |
Unit cell lengths | 76.907, 76.907, 40.298 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.670 - 2.000 |
R-factor | 0.15534 |
Rwork | 0.153 |
R-free | 0.21200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2b33 |
RMSD bond length | 0.016 |
RMSD bond angle | 1.456 |
Data reduction software | CrysalisPro |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.700 | 2.100 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.045 | 0.183 |
Number of reflections | 6001 | |
<I/σ(I)> | 16.2 | 5.5 |
Completeness [%] | 99.9 | 99.3 |
Redundancy | 3 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 298 | 18% PEG 3350, 0.1 M MES pH6.0 |