5HDW
ApaG Domain of FBxo3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 93 |
Detector technology | CCD |
Collection date | 2014-08-03 |
Detector | RAYONIX MX300-HS |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 30.477, 96.813, 40.517 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.380 - 2.000 |
R-factor | 0.2036 |
Rwork | 0.200 |
R-free | 0.23810 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1xvs |
RMSD bond length | 0.013 |
RMSD bond angle | 1.329 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.380 | |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.076 | 0.417 |
Number of reflections | 8588 | |
<I/σ(I)> | 10.3 | 2.7 |
Completeness [%] | 99.3 | 97.8 |
Redundancy | 5.41 | 5.57 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 298 | 100mM Tris-HCl pH 8.5 20% w/v PEG 8000 200mM MgCl2 * 6H2O |