5H4C

Crystal structure of Cbln4

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	CCD
Collection date	2014-10-31
Detector	RAYONIX MX-325
Wavelength(s)	0.9199
Spacegroup name	P 43 21 2
Unit cell lengths	91.198, 91.198, 148.693
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 2.300
R-factor	0.17829
Rwork	0.176
R-free	0.21359
RMSD bond length	0.016
RMSD bond angle	1.132
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	REFMAC (5.6.0117)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.300
Number of reflections	28464
<I/σ(I)>	15.8
Completeness [%]	99.8
Redundancy	9.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	298	4% Tacsimate, pH 7.0, 12% PEG 3350