5H4B

Crystal structure of Cbln4

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NFPSS BEAMLINE BL19U1
Synchrotron site	NFPSS
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2014-03-28
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	0.9788
Spacegroup name	P 43 3 2
Unit cell lengths	132.357, 132.357, 132.357
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 2.800
R-factor	0.2085
Rwork	0.207
R-free	0.23282
RMSD bond length	0.014
RMSD bond angle	1.299
Data scaling software	HKL-3000
Phasing software	PHENIX
Refinement software	REFMAC (5.6.0117)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.800
Number of reflections	10335
<I/σ(I)>	23.5
Completeness [%]	99.9
Redundancy	9.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.2	298	2.5 M NaCl, Na/K phosphate, pH6.2