5H48
Crystal structure of Cbln1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U1 |
| Synchrotron site | SSRF |
| Beamline | BL17U1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-10-31 |
| Detector | RAYONIX MX-325 |
| Wavelength(s) | 0.9199 |
| Spacegroup name | P 6 |
| Unit cell lengths | 82.981, 82.981, 50.543 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 71.860 - 2.200 |
| R-factor | 0.16476 |
| Rwork | 0.163 |
| R-free | 0.20297 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4nn0 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.567 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 71.860 |
| High resolution limit [Å] | 2.200 |
| Number of reflections | 9670 |
| <I/σ(I)> | 13.1 |
| Completeness [%] | 94.7 |
| Redundancy | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.2 M Sodium tartrate dibasic dihydrate, 20% PEG3350, pH 7.3 |
