5H1Z
CYP153D17 from Sphingomonas sp. PAMC 26605
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-04-02 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.97933 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 110.837, 110.837, 113.180 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.010 - 3.100 |
R-factor | 0.26569 |
Rwork | 0.262 |
R-free | 0.33956 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.797 |
Data scaling software | HKL-2000 |
Refinement software | REFMAC (5.8.0151) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 95.990 |
High resolution limit [Å] | 3.080 |
Number of reflections | 14358 |
<I/σ(I)> | 26.76 |
Completeness [%] | 91.3 |
Redundancy | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 23% (w/v) PEG 3350 |