Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | NSRRC BEAMLINE BL13B1 |
| Synchrotron site | NSRRC |
| Beamline | BL13B1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-07-13 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.8563, 0.9189, 0.9195 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 61.993, 61.993, 208.727 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 37.419 - 2.588 |
| R-factor | 0.2449 |
| Rwork | 0.243 |
| R-free | 0.28750 |
| Structure solution method | MAD |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.519 |
| Data scaling software | HKL-2000 |
| Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.670 |
| High resolution limit [Å] | 2.580 | 2.580 |
| Number of reflections | 7937 | |
| <I/σ(I)> | 10.3 | |
| Completeness [%] | 98.0 | 98 |
| Redundancy | 33 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6 | 277.15 | 50mM sodium cacodylate, 10mM magnesium chloride, 5mM cobalt(II) chloride, 1mM spermine, 8% MPD |
