5GTB
crystal structure of intermembrane space region of the ARC6-PDV2 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-11-09 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9796 |
Spacegroup name | H 3 2 |
Unit cell lengths | 151.228, 151.228, 100.566 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 27.438 - 2.871 |
R-factor | 0.267 |
Rwork | 0.265 |
R-free | 0.30200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5had |
RMSD bond length | 0.010 |
RMSD bond angle | 1.340 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.438 | 2.920 |
High resolution limit [Å] | 2.871 | 2.870 |
Rmerge | 0.076 | |
Number of reflections | 10239 | |
<I/σ(I)> | 33.8 | |
Completeness [%] | 93.8 | |
Redundancy | 12.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 291 | PEG2000MME, Tris pH6.5 |