5GNC

Crystal structure of Phytophthora. sojae PSR2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	CCD
Collection date	2014-11-21
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.97915
Spacegroup name	P 1 21 1
Unit cell lengths	86.320, 49.720, 94.450
Unit cell angles	90.00, 110.88, 90.00

Refinement procedure

Resolution	30.000 - 2.800
R-factor	0.2117
Rwork	0.208
R-free	0.26640
RMSD bond length	0.010
RMSD bond angle	1.128
Data scaling software	HKL-2000
Phasing software	AutoSol
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	30.000
High resolution limit [Å]	2.800
Number of reflections	18820
<I/σ(I)>	2.8
Completeness [%]	98.8
Redundancy	7.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	20% PEG 3350, 0.2M NH4COOH