Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
| Synchrotron site | PAL/PLS |
| Beamline | 7A (6B, 6C1) |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-07-29 |
| Detector | ADSC QUANTUM 270 |
| Wavelength(s) | 1.2398 |
| Spacegroup name | P 1 |
| Unit cell lengths | 40.269, 41.501, 85.091 |
| Unit cell angles | 89.99, 90.01, 98.90 |
Refinement procedure
| Resolution | 39.780 - 2.800 |
| R-factor | 0.217 |
| Rwork | 0.217 |
| R-free | 0.22700 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4xg2 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.565 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 39.780 | 2.850 |
| High resolution limit [Å] | 2.800 | 2.800 |
| Number of reflections | 12408 | |
| <I/σ(I)> | 30.18 | |
| Completeness [%] | 99.7 | |
| Redundancy | 5.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 278 | 10~20%(V/V) PEG3350, 100 MM TRIS-HCL |
