5G24
Type IV-like pilin TTHA1219 from Thermus thermophilus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 77 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 116.830, 32.170, 108.120 |
Unit cell angles | 90.00, 115.51, 90.00 |
Refinement procedure
Resolution | 97.580 - 2.300 |
R-factor | 0.19266 |
Rwork | 0.190 |
R-free | 0.24034 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5g23 |
RMSD bond length | 0.021 |
RMSD bond angle | 1.877 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 57.770 | 2.360 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.110 | 0.820 |
Number of reflections | 16586 | |
<I/σ(I)> | 14.3 | 2.6 |
Completeness [%] | 99.8 | 99.2 |
Redundancy | 8.1 | 8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.01M ZINC CHLORIDE, 0.1M SODIUM ACETATE PH 5 AND 20% (W/V) PEG 6000 |