5G23
Type IV-like pilin TTHA1219 from Thermus thermophilus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 77 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 65.400, 66.950, 97.470 |
Unit cell angles | 90.00, 99.14, 90.00 |
Refinement procedure
Resolution | 96.230 - 1.850 |
R-factor | 0.18173 |
Rwork | 0.180 |
R-free | 0.20878 |
Structure solution method | SIRAS |
Starting model (for MR) | NONE |
RMSD bond length | 0.018 |
RMSD bond angle | 1.843 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | AutoSol |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.940 | 1.900 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.080 | 0.790 |
Number of reflections | 70620 | |
<I/σ(I)> | 12.6 | 2.2 |
Completeness [%] | 99.3 | 99.8 |
Redundancy | 3.3 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.01M ZINC CHLORIDE, 0.1M SODIUM ACETATE PH 5 AND 20% (W/V) PEG 6000 |