5FVB
CRYSTAL STRUCTURE OF PHORMIDIUM C-PHYCOERYTHRIN AT PH 5.0
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | RRCAT INDUS-2 BEAMLINE PX-BL21 |
Synchrotron site | RRCAT INDUS-2 |
Beamline | PX-BL21 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-07-14 |
Detector | MARRESEARCH |
Wavelength(s) | 0.97947 |
Spacegroup name | P 1 |
Unit cell lengths | 109.165, 109.148, 117.680 |
Unit cell angles | 78.71, 82.30, 61.55 |
Refinement procedure
Resolution | 38.891 - 1.930 |
R-factor | 0.186 |
Rwork | 0.183 |
R-free | 0.23880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5aqd |
RMSD bond length | 0.007 |
RMSD bond angle | 2.127 |
Data reduction software | autoPROC |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.890 | 2.030 |
High resolution limit [Å] | 1.930 | 1.930 |
Rmerge | 0.060 | 0.200 |
Number of reflections | 338355 | |
<I/σ(I)> | 13.4 | 4.8 |
Completeness [%] | 96.2 | 92 |
Redundancy | 3.4 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5 | 0.1M CITRATE (PH 5.0), 5% PEG-6000 AND 25% GLYCEROL |