5FRA
CBM40_CPF0721-6'SL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-03-06 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 78.502, 84.267, 89.996 |
Unit cell angles | 90.00, 90.79, 90.00 |
Refinement procedure
Resolution | 39.690 - 2.000 |
R-factor | 0.18011 |
Rwork | 0.179 |
R-free | 0.21035 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2v73 |
RMSD bond length | 0.017 |
RMSD bond angle | 1.732 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.690 | 2.040 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.060 | 0.390 |
Number of reflections | 74668 | |
<I/σ(I)> | 11.8 | 3.1 |
Completeness [%] | 99.4 | 99.5 |
Redundancy | 3.7 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.5 | 25% PEG 2K MME 0.3M CH3COONA 0.1M CH3COONA PH4.5 |