5FQ6
Crystal structure of the SusCD complex BT2261-2264 from Bacteroides thetaiotaomicron
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-07-04 |
Detector | DECTRIS PILATUS |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 222.027, 91.941, 261.219 |
Unit cell angles | 90.00, 98.23, 90.00 |
Refinement procedure
Resolution | 48.799 - 2.800 |
R-factor | 0.2005 |
Rwork | 0.198 |
R-free | 0.25460 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 5FQ4 AND 5FQ3 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.080 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.800 | 2.850 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.200 | 1.310 |
Number of reflections | 256052 | |
<I/σ(I)> | 8.9 | 2.1 |
Completeness [%] | 99.6 | 99.1 |
Redundancy | 9.3 | 9.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.2 M MAGNESIUM FORMATE DIHYDRATE 0.05 M TRIS PH 8 18-22% PEG3350 |