5FHX
CRYSTAL STRUCTURE OF CODV IN COMPLEX WITH IL4 AT 2.55 Ang. RESOLUTION.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-09-26 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.967 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 77.210, 73.330, 91.400 |
| Unit cell angles | 90.00, 112.72, 90.00 |
Refinement procedure
| Resolution | 23.150 - 2.550 |
| R-factor | 0.1872 |
| Rwork | 0.184 |
| R-free | 0.24860 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.230 |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.5) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 23.150 | 2.640 |
| High resolution limit [Å] | 2.550 | 2.550 |
| Number of reflections | 30823 | |
| <I/σ(I)> | 7.6 | |
| Completeness [%] | 99.4 | 99.5 |
| Redundancy | 3.4 | 3.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 292 | PEG 3350 20%, K-Acetate 0.20M |
