5FHI

Crystallographic structure of PsoE without Co

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE BL-1A
Synchrotron site	Photon Factory
Beamline	BL-1A
Temperature [K]	100
Detector technology	PIXEL
Collection date	2015-05-30
Detector	DECTRIS EIGER X 4M
Wavelength(s)	1.10
Spacegroup name	P 65 2 2
Unit cell lengths	145.413, 145.413, 51.266
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	47.598 - 2.410
R-factor	0.1908
Rwork	0.185
R-free	0.24560
RMSD bond length	0.015
RMSD bond angle	1.448
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	AutoSol
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.410
Number of reflections	12786
<I/σ(I)>	30.54
Completeness [%]	99.8
Redundancy	19.45

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	PEGmme 5000