5FC7

Murine SMPDL3A in complex with sulfate (tetragonal)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08ID-1
Synchrotron site	CLSI
Beamline	08ID-1
Temperature [K]	100
Detector technology	CCD
Collection date	2015-01-21
Detector	RAYONIX MX-300
Wavelength(s)	0.97949
Spacegroup name	P 41
Unit cell lengths	87.385, 87.385, 79.843
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	36.312 - 1.456
R-factor	0.1541
Rwork	0.153
R-free	0.18300
RMSD bond length	0.011
RMSD bond angle	1.123
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	36.312
High resolution limit [Å]	1.456
Number of reflections	100829
<I/σ(I)>	15
Completeness [%]	96.4
Redundancy	4.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4.6	293	0.2 M (NH4)2SO4, 0.1 M sodium acetate pH 4.6, 25% PEG 4000