5FA7
CTX-M-15 in complex with FPI-1523
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CLSI BEAMLINE 08ID-1 |
| Synchrotron site | CLSI |
| Beamline | 08ID-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2015-07-15 |
| Detector | RAYONIX MX-300 |
| Wavelength(s) | 1.00 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 62.730, 60.270, 76.010 |
| Unit cell angles | 90.00, 112.78, 90.00 |
Refinement procedure
| Resolution | 33.400 - 1.670 |
| R-factor | 0.1767 |
| Rwork | 0.175 |
| R-free | 0.20650 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.120 |
| Data reduction software | xia2 |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.10.0) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 70.100 |
| High resolution limit [Å] | 1.670 |
| Number of reflections | 59836 |
| <I/σ(I)> | 12.2 |
| Completeness [%] | 98.4 |
| Redundancy | 2.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 298 | 0.2M ammonium sulfate, 0.1M MES pH6.5, 30% PEG5K monomethyl ether |
