5F9U
X-RAY STRUCTURE OF THE ADDUCT BETWEEN HEN EGG WHITE LYSOZYME AND CISPLATIN UPON 24 HOURS OF INCUBATION AT 20 DEGREES
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-10-20 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.785, 78.785, 36.975 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.710 - 1.850 |
R-factor | 0.17326 |
Rwork | 0.170 |
R-free | 0.23310 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 193l |
RMSD bond length | 0.018 |
RMSD bond angle | 1.803 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.710 | 1.880 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.123 | 0.989 |
Number of reflections | 10302 | |
<I/σ(I)> | 16.5 | 5.3 |
Completeness [%] | 98.6 | 87.7 |
Redundancy | 5.5 | 2.9 |
CC(1/2) | 0.281 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | Crystals were grown using a reservoir solution of 1.1 M NaCl, 0.1 M sodium acetate pH 4.4 and a drop of 1 uL adduct solution and 1 uL reservoir solution. |