5F8C
Rv2258c-unbound
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-04-03 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.92019 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 109.254, 140.635, 97.239 |
Unit cell angles | 90.00, 98.56, 90.00 |
Refinement procedure
Resolution | 27.250 - 1.830 |
R-factor | 0.19252 |
Rwork | 0.191 |
R-free | 0.22599 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.269 |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0124) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.250 | 1.860 |
High resolution limit [Å] | 1.830 | 1.830 |
Number of reflections | 127941 | |
<I/σ(I)> | 28.7 | 2.9 |
Completeness [%] | 99.9 | |
Redundancy | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 296 | sodium malonate, PEG 3350 |