5F8B

Crystallographic Structure of PsoE with Co

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE AR-NW12A
Synchrotron site	Photon Factory
Beamline	AR-NW12A
Temperature [K]	100
Detector technology	CCD
Collection date	2015-06-20
Detector	ADSC QUANTUM 270
Wavelength(s)	1.0
Spacegroup name	P 65 2 2
Unit cell lengths	123.331, 123.331, 75.638
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	43.626 - 2.540
R-factor	0.1969
Rwork	0.191
R-free	0.24670
RMSD bond length	0.015
RMSD bond angle	1.823
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.540
Number of reflections	21207
<I/σ(I)>	21.38
Completeness [%]	99.8
Redundancy	11.57

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	PEGmme 5000