5F13
Structure of Mn bound DUF89 from Saccharomyces cerevisiae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-11-02 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9795 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 223.035, 95.550, 78.097 |
Unit cell angles | 90.00, 105.84, 90.00 |
Refinement procedure
Resolution | 30.174 - 2.393 |
R-factor | 0.2013 |
Rwork | 0.199 |
R-free | 0.23690 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3pt1 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.632 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | MOLREP |
Refinement software | PHENIX (dev_1888) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.174 | 2.440 |
High resolution limit [Å] | 2.393 | 2.393 |
Rmerge | 0.054 | 0.540 |
Number of reflections | 60334 | |
<I/σ(I)> | 15.03 | 1.9 |
Completeness [%] | 97.1 | |
Redundancy | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 20% P3350 ,0.1 M NH4 dihydrogen Phosphate, 5mM MnCl2 |