5EZI
Crystal Structure of Fab of parasite invasion inhibitory antibody c1 - hexagonal form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 1970-01-31 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 1 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 82.700, 82.700, 361.880 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 56.154 - 1.610 |
| R-factor | 0.1961 |
| Rwork | 0.195 |
| R-free | 0.22090 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | homology model |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.887 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.900 | 1.670 |
| High resolution limit [Å] | 1.610 | 1.610 |
| Number of reflections | 96028 | |
| <I/σ(I)> | 8.54 | 0.84 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 13.8 | 16.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 295 | 1.6 M sodium citrate pH 6.5 |
