5EWU

Crystal structure of the Arabidopsis thaliana C-terminal Chlh at 1.25A

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE AR-NE3A
Synchrotron site	Photon Factory
Beamline	AR-NE3A
Temperature [K]	100
Detector technology	CCD
Collection date	2009-06-04
Detector	ADSC QUANTUM 315
Wavelength(s)	1
Spacegroup name	P 1 21 1
Unit cell lengths	69.099, 72.776, 72.911
Unit cell angles	90.00, 109.76, 90.00

Refinement procedure

Resolution	50.000 - 1.250
R-factor	0.16971
Rwork	0.169
R-free	0.18404
RMSD bond length	0.007
RMSD bond angle	1.154
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	SHARP
Refinement software	REFMAC (5.5.0109)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.250
Number of reflections	168362
<I/σ(I)>	45
Completeness [%]	89.8
Redundancy	5.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	277	PEG, NaCl