5EST

Crystallographic analysis of the inhibition of porcine pancreatic elastase by a peptidyl boronic acid: structure of a reaction intermediate

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	52.280, 57.560, 75.410
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	7.000 - 2.200 *
Rwork	0.150
RMSD bond length	0.017
RMSD bond angle	2.400
Refinement software	EREF

Data quality characteristics

	Overall
High resolution limit [Å]	2.000 *
Rmerge	0.039 *
Total number of observations	10569 *
Number of reflections	11021 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	PPE solution	1.4 (%(w/v))
2	1	reservoir	sodium phosphate	0.1 (M)
3	1	reservoir	sodium sulfate	0.1 (M)