5DDZ

Crystal structure of the RTA-c10-P2 complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RUH3R
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2014-11-24
Detector	MAR scanner 345 mm plate
Wavelength(s)	0.9792
Spacegroup name	P 41 21 2
Unit cell lengths	67.626, 67.626, 140.652
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.010 - 1.500
R-factor	0.14767
Rwork	0.146
R-free	0.17520
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2aai
RMSD bond length	0.009
RMSD bond angle	1.240
Data reduction software	HKL-2000
Data scaling software	SCALA
Phasing software	MOLREP
Refinement software	REFMAC (5.8.0103)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.010
High resolution limit [Å]	1.500
Number of reflections	52756
<I/σ(I)>	26.5
Completeness [%]	99.7
Redundancy	11.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		289	0.4 M ammonium dihydrogen phosphate