5DCN

Crystal structure of LC3 in complex with TECPR2 LIR

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	80
Detector technology	PIXEL
Collection date	2015-05-09
Detector	PSI PILATUS 6M
Wavelength(s)	0.99987
Spacegroup name	P 32 2 1
Unit cell lengths	60.705, 60.705, 99.946
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.489 - 2.000
R-factor	0.2131
Rwork	0.209
R-free	0.24730
RMSD bond length	0.003
RMSD bond angle	0.648
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	MOLREP
Refinement software	PHENIX

Data quality characteristics

	Overall
Low resolution limit [Å]	19.870
High resolution limit [Å]	2.000
Number of reflections	14950
<I/σ(I)>	24.2
Completeness [%]	99.8
Redundancy	19.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	1.8M Lithium sulphate, 0.01M Magnesium chloride, 0.05M MES monohydrate, pH5.6