5DC4
CRYSTAL STRUCTURE OF MONOBODY AS25/ABL1 SH2 DOMAIN COMPLEX, CRYSTAL A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-03-10 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97872 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 61.281, 74.928, 39.229 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 74.930 - 1.480 |
R-factor | 0.14677 |
Rwork | 0.144 |
R-free | 0.18965 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.205 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 74.930 | 1.520 |
High resolution limit [Å] | 1.480 | 1.480 |
Rmerge | 0.235 | |
Number of reflections | 30102 | |
<I/σ(I)> | 29.7 | 4.3 |
Completeness [%] | 98.2 | 95.1 |
Redundancy | 4.9 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.83 | 291 | 0.1M Imidazole pH 7.83 and 3.5M NaCl |