5D4R

Crystal Structure of AraR(DBD) in complex with operator ORE1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE BM14
Synchrotron site	ESRF
Beamline	BM14
Temperature [K]	100
Detector technology	CCD
Collection date	2012-03-09
Detector	MAR CCD 165 mm
Wavelength(s)	1
Spacegroup name	C 1 2 1
Unit cell lengths	134.081, 42.433, 67.232
Unit cell angles	90.00, 114.82, 90.00

Refinement procedure

Resolution	36.000 - 2.070
R-factor	0.1999
Rwork	0.197
R-free	0.24710
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4h0e
RMSD bond length	0.009
RMSD bond angle	1.226
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Refinement software	PHENIX (1.8.4_1496)

Data quality characteristics

	Overall
Low resolution limit [Å]	36.000
High resolution limit [Å]	2.070
Number of reflections	21116
<I/σ(I)>	10
Completeness [%]	99.2
Redundancy	4.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		295	sodium acetate, PEG 8000, Potassium chloride