5CSC

STRUCTURE OF AN OPEN FORM OF CHICKEN HEART CITRATE SYNTHASE AT 2.8 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 43
Unit cell lengths	58.850, 58.850, 259.220
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 2.800
R-factor	0.197
RMSD bond length	0.024
RMSD bond angle	3.300
Refinement software	TNT

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	2.700 *	2.700 *
Rmerge	0.139 *
Total number of observations	53801 *
Number of reflections	15130 *
Completeness [%]	62.4 *	22 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	10 (mg/ml)
2	1	drop	citrate	0.5 (M)
3	1	drop	CoA	10 (mM)
4	1	reservoir	sodium citrate	1.0 (M)