5CE7

Structure of a non-canonical CID of Ctk3

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2011-06-29
Detector	PSI PILATUS 6M
Wavelength(s)	0.97964, 0.98012 ,0.97197
Spacegroup name	P 43 21 2
Unit cell lengths	51.310, 51.310, 119.050
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	47.120 - 2.000
R-factor	0.1917
Rwork	0.189
R-free	0.24100
Structure solution method	MAD
RMSD bond length	0.008
RMSD bond angle	1.047
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	SOLVE
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	47.120		2.050
High resolution limit [Å]	2.000	8.950	2.000
Rmerge	0.077	0.022	0.456
Rmeas	0.083	0.023	0.488
Total number of observations	157934
Number of reflections	20524	233	1556
<I/σ(I)>	20.89	70.43	4.93
Completeness [%]	100.0	100	99.9
Redundancy	7.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION	4	277	PEG 6000, citric acid, lithium chloride