5C5J
Poymerase Nucleotide complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-11-05 |
Detector | MARRESEARCH |
Wavelength(s) | 0.91596 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 86.450, 57.380, 110.640 |
Unit cell angles | 90.00, 94.51, 90.00 |
Refinement procedure
Resolution | 36.909 - 2.100 |
R-factor | 0.225 |
Rwork | 0.222 |
R-free | 0.27440 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ir9 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.078 |
Data reduction software | SCALA |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.909 | 2.210 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.069 | 0.606 |
Number of reflections | 63454 | |
<I/σ(I)> | 11.2 | 2.4 |
Completeness [%] | 99.8 | 100 |
Redundancy | 4.4 | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 298 | MPD |