5BVS
Linoleate-bound pFABP4
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
| Synchrotron site | PAL/PLS |
| Beamline | 7A (6B, 6C1) |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2015-02-25 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9794 |
| Spacegroup name | P 61 |
| Unit cell lengths | 60.487, 60.487, 139.569 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 29.560 - 2.200 |
| R-factor | 0.18885 |
| Rwork | 0.187 |
| R-free | 0.22606 |
| RMSD bond length | 0.029 |
| RMSD bond angle | 2.525 |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 2.200 |
| Number of reflections | 28819 |
| <I/σ(I)> | 55.9 |
| Completeness [%] | 99.7 |
| Redundancy | 10.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M CHES (pH 9.5), 30% (w/v) PEG 3000 |
