5BP5

Crystal structure of HA17-HA33-IPT

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 24-ID-C
Synchrotron site	APS
Beamline	24-ID-C
Temperature [K]	100
Detector technology	CCD
Collection date	2013-03-21
Detector	ADSC QUANTUM 315
Wavelength(s)	0.979180
Spacegroup name	C 2 2 21
Unit cell lengths	105.868, 118.928, 162.197
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	47.950 - 2.180
R-factor	0.2274
Rwork	0.227
R-free	0.23850
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	REFMAC (5.7.0029)

Data quality characteristics

	Overall
Low resolution limit [Å]	47.950
High resolution limit [Å]	2.180
Number of reflections	53512
<I/σ(I)>	15.1
Completeness [%]	99.5
Redundancy	3.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	0.1 M MES, 0.1 M magnesium chloride, 5% PEG 8000