5AZV

Crystal structure of hPPARgamma ligand binding domain complexed with 17-oxoDHA

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE AR-NW12A
Synchrotron site	Photon Factory
Beamline	AR-NW12A
Temperature [K]	100
Detector technology	CCD
Collection date	2013-11-16
Detector	ADSC QUANTUM 4
Wavelength(s)	1.00000
Spacegroup name	C 1 2 1
Unit cell lengths	92.610, 60.950, 118.210
Unit cell angles	90.00, 102.36, 90.00

Refinement procedure

Resolution	10.000 - 2.700
R-factor	0.22541
Rwork	0.221
R-free	0.30664
RMSD bond length	0.011
RMSD bond angle	1.366
Refinement software	REFMAC (5.8.0103)

Data quality characteristics

	Overall
Low resolution limit [Å]	45.560
High resolution limit [Å]	2.700
Number of reflections	17279
<I/σ(I)>	14.7
Completeness [%]	96.4
Redundancy	3.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.4	293	0.1 M Tris-HCl, 0.825 M sodium citrate