5AZT

Ternary complex of hPPARalpha ligand binding domain, 17-oxoDHA and a SRC1 peptide

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE AR-NW12A
Synchrotron site	Photon Factory
Beamline	AR-NW12A
Temperature [K]	100
Detector technology	CCD
Collection date	2015-06-26
Detector	ADSC QUANTUM 4
Wavelength(s)	1.00000
Spacegroup name	P 41 21 2
Unit cell lengths	59.460, 59.460, 317.940
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	11.000 - 3.450
R-factor	0.25537
Rwork	0.253
R-free	0.30763
RMSD bond length	0.007
RMSD bond angle	1.257
Refinement software	REFMAC (5.8.0103)

Data quality characteristics

	Overall
Low resolution limit [Å]	47.610
High resolution limit [Å]	3.450
Number of reflections	8185
<I/σ(I)>	15.6
Completeness [%]	98.5
Redundancy	10.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.9	293	0.1M HEPES, 35% PEG3350