5APR

STRUCTURES OF COMPLEXES OF RHIZOPUSPEPSIN WITH PEPSTATIN AND OTHER STATINE-CONTAINING INHIBITORS

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	60.330, 60.640, 106.760
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.100
R-factor	0.144
RMSD bond length	0.012
RMSD bond angle	0.036
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	2.100 *
Rmerge	0.041 *
Total number of observations	65065 *
Number of reflections	23039 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	other *	6 *		grown in the cold from a filtered *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	enzyme solution	10 (mg/ml)
2	1	1	cacodylate	50 (mM)
3	1	1	calcium acetate	20 (mM)