5AOH

Crystal Structure of CarF

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	180
Detector technology	PIXEL
Collection date	2013-06-27
Detector	DECTRIS PILATUS
Spacegroup name	P 21 21 21
Unit cell lengths	49.470, 55.450, 176.200
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	88.100 - 1.800
R-factor	0.14025
Rwork	0.137
R-free	0.20813
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.021
RMSD bond angle	1.878
Data reduction software	MOSFLM
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	REFMAC (5.8.0131)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	36.130	1.840
High resolution limit [Å]	1.800	1.800
Rmerge	0.090	0.410
Number of reflections	44709
Completeness [%]	97.5	99.1
Redundancy	3.2	3.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1