5AFQ
Crystal structure of RPC62 - RPC32 beta
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2011-09-29 |
Detector | ADSC CCD |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 218.270, 218.270, 182.930 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.750 - 7.000 |
R-factor | 0.2708 |
Rwork | 0.268 |
R-free | 0.29840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2xub |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 86.000 | 7.380 |
High resolution limit [Å] | 7.000 | 7.000 |
Rmerge | 0.060 | 0.620 |
Number of reflections | 3668 | |
<I/σ(I)> | 8.1 | 1.2 |
Completeness [%] | 99.2 | 97.9 |
Redundancy | 4.9 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 100MM ADA PH 6.5, 100MM LI2SO4, 14% PEG 4000 |